Single-line diffraction and microstructural analysis of NiOxGDC(1-x) nanocomposites

Miguel Angel Niño Galeano; R. V. Mangalaraja; R. Udayabhaskar; Naveenraj Selvaraj; Jonathan Usuba; Ricardo E. Ávila; Miguel A. Gracia

doi:10.1016/j.jssc.2020.121400

Single-line diffraction and microstructural analysis of NiO_xGDC_(1-x) nanocomposites

Miguel Angel Niño Galeano, R. V. Mangalaraja, R. Udayabhaskar, Naveenraj Selvaraj, Jonathan Usuba, Ricardo E. Ávila, Miguel A. Gracia

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

Resumen

NiO_xGDC_(1-x) nanopowders were stoichiometrically prepared with x = 0 to 1 by self-sustained combustion solution method and subsequently calcined at 600 °C. The prepared samples were examined using the X-ray diffraction pattern having integral breadth (β) of reflection and analyzed using the Voigt (V) adjustment in order to characterize the microstructure in terms of the crystallite size and microstrain. The results of X-ray diffraction analysis were compared with those derived from high-resolution transmission electron microscopy.

Idioma original	Inglés
Número de artículo	121400
Publicación	Journal of Solid State Chemistry
Volumen	288
DOI	https://doi.org/10.1016/j.jssc.2020.121400
Estado	Publicada - ago. 2020
Publicado de forma externa	Sí

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10.1016/j.jssc.2020.121400

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@article{701f37608cf549a0b5cc56b4ff69e6e6,

title = "Single-line diffraction and microstructural analysis of NiOxGDC(1-x) nanocomposites",

abstract = "NiOxGDC(1-x) nanopowders were stoichiometrically prepared with x = 0 to 1 by self-sustained combustion solution method and subsequently calcined at 600 °C. The prepared samples were examined using the X-ray diffraction pattern having integral breadth (β) of reflection and analyzed using the Voigt (V) adjustment in order to characterize the microstructure in terms of the crystallite size and microstrain. The results of X-ray diffraction analysis were compared with those derived from high-resolution transmission electron microscopy.",

keywords = "Combustion synthesis, Crystallite size, HR-TEM, Microdeformation, NiO-GDC, Voigt",

author = "{Ni{\~n}o Galeano}, {Miguel Angel} and Mangalaraja, {R. V.} and R. Udayabhaskar and Naveenraj Selvaraj and Jonathan Usuba and {\'A}vila, {Ricardo E.} and Gracia, {Miguel A.}",

note = "Publisher Copyright: {\textcopyright} 2020 Elsevier Inc.",

year = "2020",

month = aug,

doi = "10.1016/j.jssc.2020.121400",

language = "English",

volume = "288",

journal = "Journal of Solid State Chemistry",

issn = "0022-4596",

publisher = "Academic Press Inc.",

}

TY - JOUR

T1 - Single-line diffraction and microstructural analysis of NiOxGDC(1-x) nanocomposites

AU - Niño Galeano, Miguel Angel

AU - Mangalaraja, R. V.

AU - Udayabhaskar, R.

AU - Selvaraj, Naveenraj

AU - Usuba, Jonathan

AU - Ávila, Ricardo E.

AU - Gracia, Miguel A.

PY - 2020/8

Y1 - 2020/8

N2 - NiOxGDC(1-x) nanopowders were stoichiometrically prepared with x = 0 to 1 by self-sustained combustion solution method and subsequently calcined at 600 °C. The prepared samples were examined using the X-ray diffraction pattern having integral breadth (β) of reflection and analyzed using the Voigt (V) adjustment in order to characterize the microstructure in terms of the crystallite size and microstrain. The results of X-ray diffraction analysis were compared with those derived from high-resolution transmission electron microscopy.

AB - NiOxGDC(1-x) nanopowders were stoichiometrically prepared with x = 0 to 1 by self-sustained combustion solution method and subsequently calcined at 600 °C. The prepared samples were examined using the X-ray diffraction pattern having integral breadth (β) of reflection and analyzed using the Voigt (V) adjustment in order to characterize the microstructure in terms of the crystallite size and microstrain. The results of X-ray diffraction analysis were compared with those derived from high-resolution transmission electron microscopy.

KW - Combustion synthesis

KW - Crystallite size

KW - HR-TEM

KW - Microdeformation

KW - NiO-GDC

KW - Voigt

UR - http://www.scopus.com/inward/record.url?scp=85084114888&partnerID=8YFLogxK

U2 - 10.1016/j.jssc.2020.121400

DO - 10.1016/j.jssc.2020.121400

M3 - Article

AN - SCOPUS:85084114888

SN - 0022-4596

VL - 288

JO - Journal of Solid State Chemistry

JF - Journal of Solid State Chemistry

M1 - 121400

ER -

Single-line diffraction and microstructural analysis of NiOxGDC(1-x) nanocomposites

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Single-line diffraction and microstructural analysis of NiO_xGDC_(1-x) nanocomposites